Dynamic freeze casting for the production of porous titanium (Ti) scaffolds

Hyun Do Jung, Se Won Yook, Tae Sik Jang, Yuanlong Li, Hyoun Ee Kim, Young-Hag Koh

Research output: Contribution to journalArticle

48 Citations (Scopus)

Abstract

This paper proposes dynamic freeze casting as a new manufacturing technique for producing porous Ti scaffolds with a uniform porous structure and good ductility. In this method, Ti/camphene slurries with various initial Ti contents (15, 20, and 25 vol.%) were frozen at 44 °C for 12 h in rotation, which allowed for the extensive growth of camphene crystals and the uniform construction of walls made of Ti particles. All the fabricated samples showed spherical-like pores surrounded by dense Ti walls that were uniformly formed after sintering at 1300 °C for 2 h in a vacuum. The porosity decreased from 71 to 52 vol.% with an increase in Ti content from 15 to 25 vol.%, whereas the pore size decreased from 362 to 95 μm. On the other hand, the compressive strength and stiffness increased considerably from 57 ± 4 to 183 ± 6 MPa and from 1.3 ± 0.5 to 5.0 ± 0.8 GPa, respectively, due to the decrease in the porosity of the samples.

Original languageEnglish
Pages (from-to)59-63
Number of pages5
JournalMaterials Science and Engineering C
Volume33
Issue number1
DOIs
Publication statusPublished - 2013 Jan 1

Fingerprint

Titanium
Scaffolds
Casting
titanium
Camphene
porosity
Porosity
slurries
compressive strength
Slurries
ductility
Compressive strength
Pore size
Ductility
stiffness
sintering
Sintering
manufacturing
Stiffness
Vacuum

Keywords

  • Freeze casting
  • Mechanical properties
  • Porous metal
  • Titanium

ASJC Scopus subject areas

  • Materials Science(all)
  • Condensed Matter Physics
  • Mechanical Engineering
  • Mechanics of Materials

Cite this

Dynamic freeze casting for the production of porous titanium (Ti) scaffolds. / Jung, Hyun Do; Yook, Se Won; Jang, Tae Sik; Li, Yuanlong; Kim, Hyoun Ee; Koh, Young-Hag.

In: Materials Science and Engineering C, Vol. 33, No. 1, 01.01.2013, p. 59-63.

Research output: Contribution to journalArticle

Jung, Hyun Do ; Yook, Se Won ; Jang, Tae Sik ; Li, Yuanlong ; Kim, Hyoun Ee ; Koh, Young-Hag. / Dynamic freeze casting for the production of porous titanium (Ti) scaffolds. In: Materials Science and Engineering C. 2013 ; Vol. 33, No. 1. pp. 59-63.
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