Lithium-halogen exchange reaction using microreaction technology

Jaehoon Choe, Jung Hyun Seo, Youngwoon Kwon, Kwang Ho Song

Research output: Contribution to journalArticle

17 Citations (Scopus)

Abstract

A two-stage continuous microreactor system was use to synthesize the materials for an organic light emitting diode. The split and recombine type of micromixers were suitable for the two-stage reaction including lithium-bromo exchange reaction. The two-stage synthesis was carried out under non-cryogenic conditions by taking full advantage of microstructured reaction systems. In a first stage, the unstable intermediate, naphthyl lithium was synthesized with maximum yield and consumed immediately in the second stage micromixer. The naphthyl-substituted anthracene was obtained with 97% purity.

Original languageEnglish
Pages (from-to)S17-S20
JournalChemical Engineering Journal
Volume135
Issue numberSUPPL. 1
DOIs
Publication statusPublished - 2008 Jan 15

Keywords

  • Bromonaphthalene
  • Electron transport layer
  • Microreaction technology

ASJC Scopus subject areas

  • Chemistry(all)
  • Environmental Chemistry
  • Chemical Engineering(all)
  • Industrial and Manufacturing Engineering

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