One-pot polyol synthesis of monosize PVP-coated sub-5 nm Fe3O4 nanoparticles for biomedical applications

Hong Ling Liu; Seung Pil Ko; Jun Hua Wu; Myung Hwa Jung; Ji Hyun Min; Ju Hun Lee; Boo Hyun An; Young Keun Kim

doi:10.1016/j.jmmm.2006.10.776

One-pot polyol synthesis of monosize PVP-coated sub-5 nm Fe₃O₄ nanoparticles for biomedical applications

Hong Ling Liu, Seung Pil Ko, Jun Hua Wu, Myung Hwa Jung, Ji Hyun Min, Ju Hun Lee, Boo Hyun An, Young Keun Kim

Department of Materials Science and Engineering

Research output: Contribution to journal › Article › peer-review

119 Citations (Scopus)

Abstract

Polyvinylpyrrolidone (PVP)-coated sub-5 nm monosize Fe₃O₄ nanoparticles were synthesized by reduction of Fe(III) acetylacetonate in the presence of PVP polymer as surfactant in one-pot polyol process. Their microstructure and magnetic properties were characterized by XRD, TEM/HRTEM and VSM. It is found that the nanoparticles have high crystallinity with distinct lattices and the magnetic measurements reveal their well-defined superparamagnetic behavior at room temperature. Such Fe₃O₄ nanoparticles with tailorable size and tunable magnetic properties are promising for biomedical applications.

Original language	English
Pages (from-to)	e815-e817
Journal	Journal of Magnetism and Magnetic Materials
Volume	310
Issue number	2 SUPPL. PART 3
DOIs	https://doi.org/10.1016/j.jmmm.2006.10.776
Publication status	Published - 2007 Mar

Keywords

FeO
Magnetic
Magnetite
Nanoparticle
Polyol synthesis
Ultrasmall size

ASJC Scopus subject areas

Electronic, Optical and Magnetic Materials
Condensed Matter Physics

Access to Document

10.1016/j.jmmm.2006.10.776

Cite this

@article{d9f2681c7c124b65a5d620dcd2bbaca3,

title = "One-pot polyol synthesis of monosize PVP-coated sub-5 nm Fe3O4 nanoparticles for biomedical applications",

abstract = "Polyvinylpyrrolidone (PVP)-coated sub-5 nm monosize Fe3O4 nanoparticles were synthesized by reduction of Fe(III) acetylacetonate in the presence of PVP polymer as surfactant in one-pot polyol process. Their microstructure and magnetic properties were characterized by XRD, TEM/HRTEM and VSM. It is found that the nanoparticles have high crystallinity with distinct lattices and the magnetic measurements reveal their well-defined superparamagnetic behavior at room temperature. Such Fe3O4 nanoparticles with tailorable size and tunable magnetic properties are promising for biomedical applications.",

keywords = "FeO, Magnetic, Magnetite, Nanoparticle, Polyol synthesis, Ultrasmall size",

author = "Liu, {Hong Ling} and Ko, {Seung Pil} and Wu, {Jun Hua} and Jung, {Myung Hwa} and Min, {Ji Hyun} and Lee, {Ju Hun} and An, {Boo Hyun} and Kim, {Young Keun}",

note = "Funding Information: This work was supported by Korea Research Foundation Grants KRF-2004-005-D00057 and KRF-2005-210-D00023, Korea Health 21 R&D Project, Ministry of Health & Welfare (No. A050750), and Korea Science and Engineering Foundation (KOSEF) grant funded by the Korea government (MOST) (No. M60501000045-05A0100-04510).",

year = "2007",

month = mar,

doi = "10.1016/j.jmmm.2006.10.776",

language = "English",

volume = "310",

pages = "e815--e817",

journal = "Journal of Magnetism and Magnetic Materials",

issn = "0304-8853",

publisher = "Elsevier",

number = "2 SUPPL. PART 3",

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TY - JOUR

T1 - One-pot polyol synthesis of monosize PVP-coated sub-5 nm Fe3O4 nanoparticles for biomedical applications

AU - Liu, Hong Ling

AU - Ko, Seung Pil

AU - Wu, Jun Hua

AU - Jung, Myung Hwa

AU - Min, Ji Hyun

AU - Lee, Ju Hun

AU - An, Boo Hyun

AU - Kim, Young Keun

N1 - Funding Information: This work was supported by Korea Research Foundation Grants KRF-2004-005-D00057 and KRF-2005-210-D00023, Korea Health 21 R&D Project, Ministry of Health & Welfare (No. A050750), and Korea Science and Engineering Foundation (KOSEF) grant funded by the Korea government (MOST) (No. M60501000045-05A0100-04510).

PY - 2007/3

Y1 - 2007/3

N2 - Polyvinylpyrrolidone (PVP)-coated sub-5 nm monosize Fe3O4 nanoparticles were synthesized by reduction of Fe(III) acetylacetonate in the presence of PVP polymer as surfactant in one-pot polyol process. Their microstructure and magnetic properties were characterized by XRD, TEM/HRTEM and VSM. It is found that the nanoparticles have high crystallinity with distinct lattices and the magnetic measurements reveal their well-defined superparamagnetic behavior at room temperature. Such Fe3O4 nanoparticles with tailorable size and tunable magnetic properties are promising for biomedical applications.

AB - Polyvinylpyrrolidone (PVP)-coated sub-5 nm monosize Fe3O4 nanoparticles were synthesized by reduction of Fe(III) acetylacetonate in the presence of PVP polymer as surfactant in one-pot polyol process. Their microstructure and magnetic properties were characterized by XRD, TEM/HRTEM and VSM. It is found that the nanoparticles have high crystallinity with distinct lattices and the magnetic measurements reveal their well-defined superparamagnetic behavior at room temperature. Such Fe3O4 nanoparticles with tailorable size and tunable magnetic properties are promising for biomedical applications.

KW - FeO

KW - Magnetic

KW - Magnetite

KW - Nanoparticle

KW - Polyol synthesis

KW - Ultrasmall size

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M3 - Article

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SP - e815-e817

JO - Journal of Magnetism and Magnetic Materials

JF - Journal of Magnetism and Magnetic Materials

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IS - 2 SUPPL. PART 3

ER -