Preparation and characterization of surface modified silica nanoparticles with organo-silane compounds

Chang Hun Lee, Sun Hee Park, Wonkeun Chung, Joong Yeon Kim, Sung Hyun Kim

Research output: Contribution to journalArticle

29 Citations (Scopus)

Abstract

In this study, surface functionalized silica nanoparticles were prepared through a continuous two-step sol-gel process. After the TEOS-derived silica particles were synthesized, silane compounds were added during the second sol-gel process without any filtration or purification processes. The introductions of the organic chains to their surfaces were measured using 13C solid-state NMR. The effects of the hydrophilicity of the organo-chains on the silica particles were evaluated and analyzed by water contact angle and water wettability tests. The differences of surface charge in the dispersion state were analyzed by measuring the zeta-potential and the variations in the charge were measured as a function of pH.

Original languageEnglish
Pages (from-to)318-322
Number of pages5
JournalColloids and Surfaces A: Physicochemical and Engineering Aspects
Volume384
Issue number1-3
DOIs
Publication statusPublished - 2011 Jul 5

Fingerprint

Silanes
Silicon Dioxide
Silica
Nanoparticles
Sol-gel process
Water
Hydrophilicity
Zeta potential
Surface charge
Contact angle
Purification
Wetting
Nuclear magnetic resonance

Keywords

  • Organo-silane compounds
  • Silica nanoparticles
  • Surface functionalized silica particles

ASJC Scopus subject areas

  • Colloid and Surface Chemistry

Cite this

Preparation and characterization of surface modified silica nanoparticles with organo-silane compounds. / Lee, Chang Hun; Park, Sun Hee; Chung, Wonkeun; Kim, Joong Yeon; Kim, Sung Hyun.

In: Colloids and Surfaces A: Physicochemical and Engineering Aspects, Vol. 384, No. 1-3, 05.07.2011, p. 318-322.

Research output: Contribution to journalArticle

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