XPS investigation of Si3N4/SiC nanocomposites prepared using a commercial polymer

Yoon Suk Oh; Woo Seok Cho; Chang Sam Kim; Dae Soon Lim; Deock Soo Cheong

doi:10.1111/j.1151-2916.1999.tb01879.x

XPS investigation of Si₃N₄/SiC nanocomposites prepared using a commercial polymer

Yoon Suk Oh, Woo Seok Cho, Chang Sam Kim, Dae Soon Lim, Deock Soo Cheong

Honorary professors

Research output: Contribution to journal › Article › peer-review

24 Citations (Scopus)

Abstract

We have synthesized Si₃N₄/SiC nanocomposites using a commercial polymer. Formation behavior of SiC nanoparticles has been studied using X-ray photoelectron spectroscopy (XPS). Based on the XPS results, we concluded that SiC nanoparticles were formed by a chemical reaction of Si provided from Si₃N₄ with free carbon obtained by pyrolysis of a polymer around 1300 °C. The presence of CN_x compounds in samples processed in an Ar atmosphere supported our explanation.

Original language	English
Pages (from-to)	1076-1078
Number of pages	3
Journal	Journal of the American Ceramic Society
Volume	82
Issue number	4
DOIs	https://doi.org/10.1111/j.1151-2916.1999.tb01879.x
Publication status	Published - 1999

ASJC Scopus subject areas

Ceramics and Composites
Materials Chemistry

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abstract = "We have synthesized Si3N4/SiC nanocomposites using a commercial polymer. Formation behavior of SiC nanoparticles has been studied using X-ray photoelectron spectroscopy (XPS). Based on the XPS results, we concluded that SiC nanoparticles were formed by a chemical reaction of Si provided from Si3N4 with free carbon obtained by pyrolysis of a polymer around 1300 °C. The presence of CNx compounds in samples processed in an Ar atmosphere supported our explanation.",

author = "Oh, {Yoon Suk} and Cho, {Woo Seok} and Kim, {Chang Sam} and Lim, {Dae Soon} and Cheong, {Deock Soo}",

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AU - Oh, Yoon Suk

AU - Cho, Woo Seok

AU - Kim, Chang Sam

AU - Lim, Dae Soon

AU - Cheong, Deock Soo

PY - 1999

Y1 - 1999

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AB - We have synthesized Si3N4/SiC nanocomposites using a commercial polymer. Formation behavior of SiC nanoparticles has been studied using X-ray photoelectron spectroscopy (XPS). Based on the XPS results, we concluded that SiC nanoparticles were formed by a chemical reaction of Si provided from Si3N4 with free carbon obtained by pyrolysis of a polymer around 1300 °C. The presence of CNx compounds in samples processed in an Ar atmosphere supported our explanation.

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